Saponification Process for Making Soap

Jan 7, 2025

Saponification: The Process of Making Soap

Required Materials

  • Measuring cylinders
  • Common salt
  • Glass beakers
  • Coconut oil
  • 20% NaOH solution
  • Bunsen burner
  • Funnel
  • Filter paper
  • Glass rod
  • Spatula
  • Knife
  • Red and blue litmus papers

Procedure

Mixing Ingredients

  1. Measure Coconut Oil

    • Measure 25 ml of coconut oil using a measuring cylinder.
    • Pour the oil into a glass beaker.
  2. Add NaOH Solution

    • Use another measuring cylinder to measure 30 ml of 20% NaOH solution.
    • Pour the NaOH solution into the beaker containing coconut oil.
    • Stir the mixture vigorously with a glass rod.
  3. Observe Exothermic Reaction

    • Touch the beaker from the outside to feel the warmth.
    • The warmth indicates an exothermic reaction between coconut oil and sodium hydroxide.

Heating and Forming Soap

  1. Heat the Mixture

    • Place the beaker on a Bunsen burner.
    • Continue heating until the mixture turns into a whitish paste.
    • The mixture will contain soap in suspension form and glycerol.
  2. Cool the Mixture

    • Remove the beaker from the flame and let it cool.

Testing and Precipitating Soap

  1. Test with Litmus Paper

    • Dip red litmus paper into the suspension; it turns blue indicating a basic solution.
    • Dip blue litmus paper into the suspension; it remains unchanged indicating no acidity.
  2. Precipitate Soap

    • Add 15 grams of common salt to the suspension.
    • Stir well with a glass rod.
    • Observe that soap precipitates as a solid.

Filtering and Forming Soap

  1. Filter the Soap

    • Use filter paper fixed in a funnel to filter the mixture.
    • Pour the beaker contents over the glass rod into the funnel.
    • Soap remains on the filter paper.
  2. Dry and Shape Soap

    • Remove the soap from the funnel with a spatula onto another filter paper.
    • Dry the soap by pressing it with another filter paper.
    • Cut the dried soap into desired shapes with a knife.

Conclusion

  • Soap is successfully prepared through the saponification process by an exothermic reaction of coconut oil and NaOH, followed by precipitation and filtration.