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Salt Formation and Preparation Methods

Sep 9, 2025

Overview

This lecture covers the definition and properties of salts in chemistry, rules for salt solubility, and the three main methods to prepare salts, with a focus on the double decomposition (precipitation) method.

Definition of Salts

  • In chemistry, a salt is an ionic compound formed when the H+ ion of an acid is replaced by a metal or ammonium ion.
  • Table salt (sodium chloride) is just one kind of salt; many others exist with different ions.
  • Salts are formed by the reaction of acids with bases, metals, or ammonium ions.

Solubility Rules for Salts

  • Nitrates, sodium, potassium, and ammonium salts are always soluble in water.
  • Most sulfates are soluble except those of lead (PbSO₄), barium (BaSO₄), and calcium (CaSO₄), which are insoluble.
  • Most chlorides are soluble, except those of silver (AgCl), lead (PbCl₂), and mercury (Hg₂Cl₂).
  • Most carbonates and hydroxides are insoluble except those of sodium, potassium, and ammonium.

Methods for Preparing Salts

  • There are three main methods to make salts: double decomposition (precipitation), titration, and direct acid-base (neutralization) reaction.
  • Choosing the method depends on whether the target salt is soluble or insoluble, and whether it contains group 1 ions (spa: sodium, potassium, ammonium).
  • Use double decomposition (precipitation) to prepare insoluble salts.
  • Use titration for soluble salts containing sodium, potassium, or ammonium.
  • Use neutralization for other soluble salts.

Double Decomposition (Precipitation) Method

  • Mix two soluble salts so their ions exchange partners, producing an insoluble salt (precipitate) and a soluble byproduct.
  • The insoluble salt forms as a solid at the bottom of the container.
  • Filter the mixture to separate the solid (desired salt) from the liquid.
  • Wash the solid with distilled water to purify it, then dry it between filter papers (compression method).

Worked Examples

  • Example 1: To make lead(II) sulfate (PbSO₄), mix lead(II) nitrate and sodium sulfate, which react to precipitate PbSO₄.
  • Example 2: To make magnesium carbonate, mix magnesium nitrate and potassium carbonate, which react to give insoluble MgCO₃.

Salt Preparation Strategy

  • Step 1: Decide on the correct preparation method using the solubility rules and a flow chart.
  • Step 2: Choose the appropriate reactants (soluble salts that yield the desired ions).
  • Step 3: Write and balance the chemical equation for the reaction.
  • Step 4: Draw diagrams or sequence drawings to visualize and plan each step.
  • Step 5: Convert diagrams into clear written steps for procedures.

Key Terms & Definitions

  • Salt — An ionic compound formed when the H+ of an acid is replaced by a metal or ammonium ion.
  • Solubility — The ability of a substance to dissolve in water.
  • Precipitate — An insoluble solid formed from the reaction of two solutions.
  • Double decomposition — A method where two soluble salts react to form an insoluble salt and a soluble byproduct.
  • SPA — Abbreviation for sodium, potassium, and ammonium; indicates high solubility in their salts.

Action Items / Next Steps

  • Practice identifying suitable salt preparation methods for various salts.
  • Complete exercises on the double decomposition method.
  • Next lesson: Learn preparation details for titration and neutralization methods.