Overview
This lecture explains how ICP-OES spectrometers, such as the SPECTRO ARCOS, analyze the elemental composition of substances with high precision.
Purpose of ICP-OES Spectrometer
- Used to analyze and determine the elemental composition of sample solutions.
- Converts a sample solution into light and then quantifies the elements present using the light's properties.
Working Principle of ICP-OES
- The sample solution is introduced into a peristaltic pump.
- The sample passes into a nebulizer, transforming it into an aerosol.
- In the spray chamber, larger droplets are removed, leaving fine droplets for analysis.
- The fine aerosol enters an extremely hot plasma, causing atoms and ions to emit light at characteristic wavelengths.
- Optical components capture and disperse this emitted light into individual spectral lines.
Measurement and Data Analysis
- The intensity of emitted light at specific wavelengths correlates with the concentration of each element.
- A sealed, high-resolution optical system records the dispersed light on a detector array.
- Computer software translates recorded wavelengths and their intensities into precise elemental concentrations.
Applications and Suitability
- ICP-OES spectrometers provide highly accurate and reliable elemental analysis.
- Advanced models like the SPECTRO ARCOS are ideal for high-throughput laboratory settings due to their reliability and accuracy.
Key Terms & Definitions
- ICP-OES (Inductively Coupled Plasma Optical Emission Spectrometry) — a technique for detecting and measuring elements using light emitted from a plasma.
- Plasma — an extremely hot, ionized gas used to excite atoms so they emit light.
- Nebulizer — a device that converts liquid samples into an aerosol for introduction to the plasma.
- Spectral Line — a specific wavelength of light emitted by an element’s atoms or ions.
- Detector Array — an electronic device that records the light emitted at different wavelengths.
Action Items / Next Steps
- Review the working steps of ICP-OES for better understanding.
- Familiarize yourself with key terms and process descriptions for future reference.