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Separation Techniques: Salt and Sand Lab

Aug 17, 2024

Salt and Sand Mixture Lab Notes

Objective

  • Separate a heterogeneous mixture of salt and sand.
  • Determine the percentage of salt and sand in the mixture.

Materials Used

  • Evaporating dish
  • Wash cloth
  • Balance for weighing
  • Beaker
  • Filter paper
  • Funnel
  • Erlenmeyer flask
  • Bunsen burner
  • Water

Procedure Overview

  1. Initial Measurements

    • Mass of empty evaporating dish and watch glass: 80.67 g.
    • Mass of salt and sand mixture: 88.39 g.
  2. Dissolving the Salt

    • Add about 10 mL of water to the salt and sand mixture.
    • Salt dissolves in water; sand does not.
  3. Filtration

    • Set up filtration apparatus with funnel and Erlenmeyer flask.
    • Fold filter paper to create a filter.
    • Pour salt water through the filter, capturing sand.
    • Wash the sand with an additional 10 mL of water to ensure all salt is dissolved.
    • Observe that the sand is retained in the filter, while the salt water passes through to the beaker.
  4. Separating Salt from Water

    • Pour the salt water into the evaporating dish.
    • Cover with a watch glass and heat over a Bunsen burner.
    • Water will evaporate due to its low boiling point, leaving salt behind.
    • Wait until all water evaporates.
  5. Final Measurement

    • Final mass of the evaporating dish with salt: 83.69 g.

Calculations

  • Mass of Salt: 83.69 g (final mass) - 80.67 g (mass of dish) = 3.02 g
  • Mass of Sand: 88.39 g (initial mass) - 3.02 g (mass of salt) = 85.37 g
  • Calculate percentage of salt and sand:
    • Percentage of Salt = (3.02 g / 88.39 g) * 100
    • Percentage of Sand = (85.37 g / 88.39 g) * 100

Key Concepts

  • Heterogeneous Mixture: Mixture where components can be easily distinguished.
  • Physical Properties Used for Separation:
    • Solubility: Salt dissolves in water; sand does not.
    • Boiling Point: Water evaporates at a lower temperature than salt.

Conclusion

  • The separation of salt and sand was accomplished using differences in physical properties: solubility and boiling point.