Understanding Retardation Factor in Chromatography

Apr 26, 2025

Retardation Factor in Chromatography

Overview

  • Retardation Factor (R): Fraction of an analyte in the mobile phase of a chromatographic system.
  • Planar Chromatography Specifics (RF): Defined as the ratio of the distance traveled by the center of a spot to the distance traveled by the solvent front.
  • Relation to Retention Factor: Sometimes used synonymously but actually distinct.

General Definition

  • Formula:
    • ( R = \frac{\text{quantity of substance in the mobile phase}}{\text{total quantity of substance in the system}} )
  • Represents the fraction of the sample in the mobile phase at equilibrium.

Planar Chromatography

  • Application: Used in paper chromatography and thin-layer chromatography (TLC).
  • Formula for RF:
    • ( R_F = \frac{\text{migration distance of substance}}{\text{migration distance of solvent front}} )
  • RF Value Characteristics:
    • Always between 0 and 1.
    • Depends on the polarity of the mobile phase.
    • Characteristic for each compound under specific conditions.
    • Used for identification by comparing with known standards on a single plate.

Relationship with Retention Factor

  • Retention Factor (k):
    • Defined in column chromatography as the ratio of the time an analyte is retained in the stationary phase to the time in the mobile phase.
  • Inverse Relationship:
    • ( R = \frac{1}{1 + k} )
    • ( k = \frac{1 - R}{R} )

References

  • Information adapted from the IUPAC Compendium of Chemical Terminology, specifically regarding terms used in chromatography.

Additional Chromatography Techniques

  • Affinity Chromatography
  • Gas Chromatography
  • High-performance Liquid Chromatography
  • Thin-layer Chromatography

Prominent Publications

  • Biomedical Chromatography
  • Journal of Chromatography A
  • Journal of Chromatography B