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Hello Alkanes and Arenes: Preparation Methods

Jul 17, 2024

Lecture Notes: Hello Alkanes and Hello Arenes

Introduction

  • Welcome and enthusiasm for preparation
  • TodayтАЩs lecture will cover Hello Alkanes and Hello Arenes
  • Objective: Bring a smoky flare to life

Hello Alkanes and Hello Arenes

First Method: Preparation from Alcohol

  • Reaction: Alcohol with HX
  • Reaction Formation
    • ROH + HX --> RX + H2O
    • Organic framework alteration with halogen addition
  • Organic Rearrangement Possibilities
    • 123 Hydride shift and Methyl shift expansion

Second Method: Preparation from Silver Salts of Fatty Acids

  • Reaction: With Ethanoyl Chloride
  • Reaction Formation
    • R-COOAg + Cl2 --> RCl + CO2 + AgCl

Preparation from Alkyl halides (Sandmeyer Reaction)

  • Reaction: RN2+X-
    • Cu2Cl2/HCl or Cu2Br2/HBr
    • RN2+X- --> RX + N2 (gas)
    • Example: C6H5N2+Cl- + Cu2Cl2/HCl --> C6H5Cl + N2

Important Points on Reactions

  • Rearrangement in Reactions
    • Some reactions may involve rearrangement like Hydride shift, and Methyl shift.
  • Protonation step
    • Protonation is crucial for certain reactions involving alcohols.
  • Use of Protective Groups
    • Some reactions utilize protective groups for selective transformations.

Famous Reactions

SN1 (Substitution Nucleophilic Unimolecular)

  • First Step: Formation of carbocation, slow and reversible.
  • Second Step: Nucleophile attacks the carbocation, fast.
  • Rate: Depends on the stability of the carbocation.
  • Stereochemical Outcome: Racemization of configuration due to planar intermediate.

SN2 (Substitution Nucleophilic Bimolecular)

  • Reaction Mechanism: Backside attack by nucleophile.
  • Stereochemical Outcome: Inversion of configuration.
  • Rate Determining Step: One-step process involving both substrate and nucleophile.
  • Example: CH3-Cl + OH- --> CH3OH + Cl-

Commonly Used Reagents

  • Preparation of RX from ROH
    • HX (acid halides), PCl5, SOCl2
  • Sandmeyer Reaction
    • Cu2Cl2/HCl, Cu2Br2/HBr for C6H5X formation

Problem Solving Examples:

Example 1: Conversion of Benzoic Acid to Benzyl Chloride.

  • Reagents: SOCl2, Nucleophilic substitution to form benzyl chloride.

Example 2: Nitration of Chlorobenzene

  • Reagents: HNO3, H2SO4
  • Product: o-Nitrochlorobenzene, p-Nitrochlorobenzene

Notes on Complex Examples

Side Reactions and By-products

  • By-products in reactions with different conditions and reagents

Reaction Sequence Analysis

  • Detailed steps for complex reaction mechanisms

Conclusion

  • Revision and clarification of possible doubts
  • Next Lecture: Regular revision and exam preparation

Tips for Quick Revision:

  • Use flowcharts for mechanisms
  • Summarize key points for each reaction type

Summary

  • Thorough understanding of reaction mechanisms and preparations
  • Importance of identifying and handling rearrangements and protective groups

Practice regularly and keep revising important examples.