Carboxylic Acid Derivatives & Hydrolysis Reactions

Aug 8, 2025

Overview

This lecture covers carboxylic acid derivatives, their reactivity, and major reactions such as nucleophilic acyl substitution and hydrolysis, with biological and industrial examples.

Vitamin C and Esters in Biology

  • Esters are found in perfumes, fruit scents, and key biomolecules like vitamin C (ascorbic acid).
  • Vitamin C acts as an antioxidant and is essential for collagen synthesis.
  • Vitamin C deficiency causes scurvy, prevented by citrus fruits due to their vitamin C content.

Carboxylic Acid Derivatives and Reactivity

  • Four main carboxylic acid derivatives: acid chlorides, anhydrides, esters, and amides.
  • Reactivity is influenced by inductive effects (electron withdrawal) and resonance effects (electron donation).
  • Acid chlorides are the most reactive due to strong inductive effects and poor resonance stabilization.
  • Anhydrides are less reactive than acid chlorides, followed by esters, with amides being the least reactive due to strong resonance.

Nucleophilic Acyl Substitution Reactions

  • Carboxylic acid derivatives undergo nucleophilic acyl substitution via an addition-elimination mechanism.
  • Unlike aldehydes and ketones, these derivatives have good leaving groups that facilitate substitution.
  • Reactions are significant in making plastics (like nylon) and biological molecules (like proteins and fats).

Hydrolysis of Carboxylic Acid Derivatives

  • Hydrolysis breaks carboxylic acid derivatives into carboxylic acids or their salts.
  • Acid chlorides and anhydrides hydrolyze with just water; esters and amides need acid or base catalysis.
  • Base-catalyzed ester hydrolysis (saponification) produces soap by forming carboxylate ions.
  • Acid-catalyzed hydrolysis avoids forming unstable negative charges and leads to alcohol and carboxylic acid products.

Biological and Industrial Examples

  • Triglycerides (fats) are made from glycerol and carboxylic acids, linked by ester bonds.
  • Ester hydrolysis is essential in digestion (catalyzed by lipase) and soap-making.
  • Acid and base hydrolysis mechanisms differ in intermediates and leaving groups.

Hydrolysis in Synthesis

  • Acid-catalyzed hydrolysis is used in penicillin synthesis to convert esters or amides to carboxylic acids or amines.
  • Protecting groups (like tert-butyl esters) can be added and later removed by hydrolysis during synthesis.

Key Terms & Definitions

  • Ester — a compound formed from an acid and an alcohol, containing the –COOR group.
  • Carboxylic Acid Derivative — compounds derived from carboxylic acids (acid chlorides, anhydrides, esters, amides).
  • Inductive Effect — electron withdrawal through sigma bonds by electronegative atoms.
  • Resonance Effect — delocalization of electrons that stabilizes molecules.
  • Nucleophilic Acyl Substitution — reaction where a nucleophile replaces a leaving group on an acyl compound.
  • Hydrolysis — reaction with water that breaks bonds, converting derivatives to carboxylic acids/salts.
  • Saponification — base-catalyzed hydrolysis of esters to make soap.

Action Items / Next Steps

  • Review mechanisms of acid- and base-catalyzed hydrolysis for esters and amides.
  • Prepare for the next lecture on interconversion of carboxylic acid derivatives.